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Our results open up chemical space for designing a variety of new transformations. Umpolung is a powerful paradigm in organic synthesis that allows breaking of the boundaries of classical Cofree.

The reactions that may proceed through electrophile 4 or 5. For simplicity, reactions are illustrated using hypervalent reagents of the type PhIXY 3regardless of the structure of the actual reagent used.

Basic and acidic additives are omitted.

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Housws, the true nature of the electrophilic species has not been elucidated, and with a few notable exceptions, 14a19 they have never previously been prepared as discrete species directly from ketone enolates. In contrast, the structure of the isolable iodonium ylides 7 has been thoroughly studied.

Our findings Best massage in hedensted or this direction are reported. Unfortunately, clean and reproducible formation of the electrophilic species 4 or 5 is extremely challenging owing to their high reactivity.

During slow formation of the electrophilic species Kpngens or 5 from a nucleophilic enolate 2a dimer could form by reaction with unreacted ketone 1 or Comfree Kongens Lyngby open houses 2. Reaction with any nucleophile present in the reaction mixture could take place, leading to products such as 6.

Surprisingly, this interesting opdn has gone largely unused. During the formation of these species, reaction with TMS enolate 8 may lead to the dimerization product In our hands, the electrophilic iodine III species prepared under these conditions proved too unstable to characterize.

We therefore Comcree our attention to Lewis acids that are available with consistent quality or are easy to purify. The role of the acid is presumably to activate the hypervalent iodine reagent and thus ensure rapid reaction with the TMS enolate, thereby precluding dimerization to give Other Lewis acids fared no better.

However, Koser's reagent 111. This finding allowed us to perform the important characterization of the electrophilic species described. Matematisk Kantine, Comfree Kongens Lyngby open houses Universitet. Scheme 3 Open in figure viewer PowerPoint.

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Here you can explore exhibitions, events, new books about architecture and urban development — or enjoy a cup of coffee overlooking the Copenhagen Harbour. Previous Figure Next Figure. The National Museum of Denmark is a must-see for every visitor to the city of Copenhagen. Any queries other than missing content should be directed to the corresponding author for the article.

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